Carlo CRESCENZI | ANALYTICAL CHEMISTRY
Carlo CRESCENZI ANALYTICAL CHEMISTRY
cod. 0760200010
ANALYTICAL CHEMISTRY
| 0760200010 | |
| DIPARTIMENTO DI FARMACIA | |
| EQF7 | |
| PHARMACEUTICAL CHEMISTRY AND TECHNOLOGY | |
| 2019/2020 |
| OBBLIGATORIO | |
| YEAR OF COURSE 2 | |
| YEAR OF DIDACTIC SYSTEM 2016 | |
| PRIMO SEMESTRE |
| SSD | CFU | HOURS | ACTIVITY | |
|---|---|---|---|---|
| CHIM/01 | 5 | 40 | LESSONS |
| Objectives | |
|---|---|
| THE STUDENT AT THE END OF THE COURSE SHOULD DEMONSTRATE HIS GENERAL KNOWLEDGE OF QUALITATIVE AND QUANTITATIVE ANALYSIS METHODS. IN DETAILS: HE SHOULD BE ABLE OF -DESCRIBING THE DIFFERENT STEPS OF AN ANALYTICAL PROCEDURE WITH SPECIAL CONCERN ON THE ANALYSIS OF THE DATA AND THEIR RELIABILITY; - USING GRAVIMETRIC AND VOLUMETRIC METHODS AS WELL AS ARRANGING THE STECHIOMETRIC CALCULATION NEEDED FOR THEIR USE; - DESIGNING THE USE OF EXTRACTION, SEPARATION AND PURIFICATION TECHNIQUES WITH PARTICULAR REFERENCE TO THE VARIOUS CHROMATOGRAPHIC METHODS; - READING A CHROMATOGRAM FOR QUALITATIVE AND QUANTITATIVE ANALYSIS AND EVALUATING SEPARATION EFFICIENCY. |
| Prerequisites | |
|---|---|
| TO GAIN ACCESS TO THE EXAM, THE STUDENT MUST HAVE PASSED THE EXAMINATION OF GENERAL AND INORGANIC CHEMISTRY. APPROPRIATE PROFICIENCY IN BASIC MATHEMATICS, PHYSICS AND STOICHIOMETRY AS WELL AS SOME KNOWLEDGE OF ORGANIC CHEMISTRY ARE ALSO REQUIRED. |
| Contents | |
|---|---|
| BASIC CONCEPTS OF ANALYTICAL CHEMISTRY FIGURE OF MERITS AND RELIABILITY: SENSITIVITY, SELECTIVITY, DYNAMIC RANGE, ROBUSTNESS, ACCURACY, PRECISION, TRUENESS. RECOVERY AND DILUTION TESTS. STATISTICAL ASSESSMENT AND TREATMENT OF EXPERIMENTAL DATA. ERRORS; UNIVARIATE ANALYSIS; TESTS OF SIGNIFICANCE, T-TEST, F TEST, DIXON TEST (OR Q-TEST); CALIBRATION METHODS: EXTERNAL STANDARDS, INTERNAL STANDARDS, STANDARD ADDITION; VARIABLE CORRELATION AND REGRESSION; INTRODUCTION TO MULTIVARIATE ANALYSIS. CHEMICAL EQUILIBRIA IN ANALYTICAL CHEMISTRY ACTIVITY AND CONCENTRATION, IONIC STRENGTH. EQUILIBRIA IN SOLUTION. ACID-BASE TITRATIONS; COMPLEXOMETRIC TITRATIONS; PRECIPITATION TITRATIONS; REDOX TITRATIONS. GRAVIMETRIC TECHNIQUES OF ANALYSIS. BASIC CONCEPTS ON INSTRUMENTAL ANALYTICAL TECHNIQUES THE ANALYTICAL SIGNAL, QUALITATIVE AND QUANTITATIVE ASPECTS. SPECTROSCOPIC TECHNIQUES: DEFINITION OF ELECTROMAGNETIC RADIATION. INTERACTION BETWEEN ELECTROMAGNETIC RADIATIONS AND MATTER: ABSORPTION AND EMISSION, ENERGY LEVELS AND TRANSITIONS. QUALITATIVE AND QUANTITATIVE ASPECTS: ABSORPTION AND EMISSION SPECTRA; LAMBERT-BEER'S LAW. UV-VIS AND IR SPECTROSCOPY. ATOMIC ABSORPTION SPECTROSCOPY. REFLECTANCE SPECTROSCOPY. SEPARATIONS TECHNIQUES: LIQUID-LIQUID EXTRACTION. SOLID PHASE EXTRACTION. SUPERCRITICAL FLUID EXTRACTION. CHROMATOGRAPHY THE PRINCIPLES OF CHROMATOGRAPHY. LIQUID CHROMATOGRAPHY. GAS CHROMATOGRAPHY. HYPHENATION OF CHROMATOGRAPHY AND MASS SPECTROMETRY. PLANAR CHROMATOGRAPHY. SHORT INTRODUCTION TO ELECTROANALYTICAL METHODS ELECTROCHEMICAL CELLS. POTENTIOMETRY. VOLTAMMETRY. CONDUCTIMETRY. |
| Teaching Methods | |
|---|---|
| - LECTURES - CLASSWORK |
| Verification of learning | |
|---|---|
| WRITTEN EXAMINATION ORAL EXAMINATION |
| Texts | |
|---|---|
| HARRIS DANIEL C. CHIMICA ANALITICA QUANTITATIVA, ZANICHELLI. SKOOG D. A, WEST D. M. & HOLLER F. J., FONDAMENTI DI CHIMICA ANALITICA, EDISES. KELLNER, MERMER, OTTO, WIDMER, CHIMICA ANALITICA, EDISES CHRISTIAN G.D. CHIMICA ANALITICA, PICCIN, PADOVA. COURSE MATERIALS |
| More Information | |
|---|---|
| . |
BETA VERSION Data source ESSE3 [Ultima Sincronizzazione: 2021-02-19]
