Carlo CRESCENZI | ANALYTICAL CHEMISTRY AND INTRODUCTION TO DRUG ANALYSIS
Carlo CRESCENZI ANALYTICAL CHEMISTRY AND INTRODUCTION TO DRUG ANALYSIS
cod. 0760100064
ANALYTICAL CHEMISTRY AND INTRODUCTION TO DRUG ANALYSIS
| 0760100064 | |
| DIPARTIMENTO DI FARMACIA | |
| EQF7 | |
| PHARMACY | |
| 2019/2020 |
| OBBLIGATORIO | |
| YEAR OF COURSE 2 | |
| YEAR OF DIDACTIC SYSTEM 2016 | |
| PRIMO SEMESTRE |
| SSD | CFU | HOURS | ACTIVITY | ||
|---|---|---|---|---|---|
| CHIMICA ANALITICA MODULO DI CHIMICA ANALITICA E INTRODUZIONE ALL'ANALISI DEI FARMACI | |||||
| CHIM/01 | 6 | 48 | LESSONS | ||
| LAB. INTRODUTTIVO ALL'ANALISI DEI FARMACI MODULO DI CHIMICA ANALITICA E INTRODUZIONE ALL'ANALISI DEI FARMACI | |||||
| CHIM/08 | 5 | 40 | LAB | ||
| Objectives | |
|---|---|
| THE OVERALL GOALS OF THIS COURSE ARE TO PROVIDE THE BASIC KNOWLEDGE REGARDING THE IONIC EQUILIBRIA IN AQUEOUS SOLUTIONS, THE PRINCIPALS OF QUALITATIVE AND QUANTITATIVE ANALYSIS, THE DIFFERENT STEPS OF A MODERN ANALYTICAL PROCEDURE AND ESPECIALLY TO THE INTERPRETATION AND STATISTICAL PROCESSING OF MEASUREMENTS. AFTER THE COURSE THE STUDENT SHOULD BE ABLE TO CORRECTLY APPLY THE THEORETICAL PRINCIPALS WHEN USING CLASSICAL WET CHEMICAL PROCEDURES AS WELL AS MODERN INSTRUMENTAL METHODS. SPECIAL ATTENTION WILL BE PAID TO VOLUMETRIC AND GRAVIMETRIC ANALYSIS, SPECTROSCOPIC AND SEPARATION TECHNIQUES WITH FOCUS ON CHROMATOGRAPHY AND THE INTERPRETATION OF CHROMATOGRAMS. |
| Prerequisites | |
|---|---|
| TO GAIN ACCESS TO THE EXAM, THE STUDENT MUST HAVE PASSED THE EXAMINATION OF GENERAL AND INORGANIC CHEMISTRY. APPROPRIATE PROFICIENCY IN BASIC MATHEMATICS, PHYSICS AND STOICHIOMETRY AS WELL AS SOME KNOWLEDGE OF ORGANIC CHEMISTRY ARE ALSO REQUIRED. |
| Contents | |
|---|---|
| BASIC CONCEPTS OF ANALYTICAL CHEMISTRY FIGURE OF MERITS AND RELIABILITY: SENSITIVITY, SELECTIVITY, DYNAMIC RANGE, ROBUSTNESS, ACCURACY, PRECISION, TRUENESS. RECOVERY AND DILUTION TESTS. STATISTICAL ASSESSMENT AND TREATMENT OF EXPERIMENTAL DATA. ERRORS; UNIVARIATE ANALYSIS; TESTS OF SIGNIFICANCE, T-TEST, F TEST, DIXON TEST (OR Q-TEST); CALIBRATION METHODS: EXTERNAL STANDARDS, INTERNAL STANDARDS, STANDARD ADDITION; VARIABLE CORRELATION AND REGRESSION; INTRODUCTION TO MULTIVARIATE ANALYSIS. CHEMICAL EQUILIBRIA IN ANALYTICAL CHEMISTRY ACTIVITY AND CONCENTRATION, IONIC STRENGTH. EQUILIBRIA IN SOLUTION. ACID-BASE TITRATIONS; COMPLEXOMETRIC TITRATIONS; PRECIPITATION TITRATIONS; REDOX TITRATIONS. GRAVIMETRIC TECHNIQUES OF ANALYSIS. BASIC CONCEPTS ON INSTRUMENTAL ANALYTICAL TECHNIQUES THE ANALYTICAL SIGNAL, QUALITATIVE AND QUANTITATIVE ASPECTS. SPECTROSCOPIC TECHNIQUES: DEFINITION OF ELECTROMAGNETIC RADIATION. INTERACTION BETWEEN ELECTROMAGNETIC RADIATIONS AND MATTER: ABSORPTION AND EMISSION, ENERGY LEVELS AND TRANSITIONS. QUALITATIVE AND QUANTITATIVE ASPECTS: ABSORPTION AND EMISSION SPECTRA; LAMBERT-BEER'S LAW. UV-VIS AND IR SPECTROSCOPY. ATOMIC ABSORPTION SPECTROSCOPY. REFLECTANCE SPECTROSCOPY. SEPARATIONS TECHNIQUES: LIQUID-LIQUID EXTRACTION. SOLID PHASE EXTRACTION. SUPERCRITICAL FLUID EXTRACTION. CHROMATOGRAPHY THE PRINCIPLES OF CHROMATOGRAPHY. LIQUID CHROMATOGRAPHY. GAS CHROMATOGRAPHY. HYPHENATION OF CHROMATOGRAPHY AND MASS SPECTROMETRY. PLANAR CHROMATOGRAPHY. SHORT INTRODUCTION TO ELECTROANALYTICAL METHODS ELECTROCHEMICAL CELLS. POTENTIOMETRY. VOLTAMMETRY. CONDUCTIMETRY. CHEMISTRY LABORATORY SAFETY RULES. PERIODIC TABLE. ACIDS BASES SALTS. SOLUTION AEQUILIBRIUM. ORGANOLECTIC PROPERTIES OF INORGANIC DRUGS. QUALITATIVE TESTS TO IDENTIFY INORGANIC DRUGS |
| Teaching Methods | |
|---|---|
| -LECTURES - LAB PRATICAL LESSONS |
| Verification of learning | |
|---|---|
| WRITTEN EXAMINATION LAB PRATICAL EXAMINATION ORAL EXAMINATION |
| Texts | |
|---|---|
| HARRIS DANIEL C. CHIMICA ANALITICA QUANTITATIVA, ZANICHELLI. SKOOG D. A, WEST D. M. & HOLLER F. J., FONDAMENTI DI CHIMICA ANALITICA, EDISES. KELLNER, MERMER, OTTO, WIDMER, CHIMICA ANALITICA, EDISES CHRISTIAN G.D. CHIMICA ANALITICA, PICCIN, PADOVA. COURSE MATERIALS |
| More Information | |
|---|---|
THE COURSE IS TAUGHT IN ITALIAN THE ATTENDANCE IS MANDATORY LOCATION: DEPARTMENT OF PHARMACY |
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