2. Professors
  3. DE RICCARDIS Francesco
  4. Teaching

INSTRUMENTAL ORGANIC ANALYSIS

Francesco DE RICCARDIS INSTRUMENTAL ORGANIC ANALYSIS

0512400021
DEPARTMENT OF CHEMISTRY AND BIOLOGY "ADOLFO ZAMBELLI"
EQF6
CHEMISTRY
2017/2018

OBBLIGATORIO
YEAR OF COURSE 2
YEAR OF DIDACTIC SYSTEM 2016
SECONDO SEMESTRE
CFUHOURSACTIVITY
432LESSONS
224EXERCISES
FRANCESCO DE RICCARDIS T Curriculum
Objectives
THE AIM OF THIS COURSE IS TO TEACH HOW TO SOLVE SIMPLE STRUCTURAL PROBLEMS BY USING THE MAJOR SPECTROSCOPIC TECHNIQUES (UV, NMR AND MS). AT THE END OF THE CLASS THE STUDENT WILL BE ABLE TO INTERPRET SPECTRA AND ASSESS THE STRUCTURE OF THE MOLECULES
Prerequisites
BASIC NOTIONS OF ORGANIC CHEMISTRY
Contents
GENERAL PRINCIPLES OF SPECTROSCOPY. NUCLEAR MAGNETIC RESONANCE. INTRODUCTION. ATOM AND NUCLEI PROPERTIES, 1H-NMR AND SPECIAL TECHNIQUES FOR 1H-NMR. 13C-NMR AND SPECIAL TECHNIQUES FOR 13C-NMR. MASS SPECTROMETRY. INTRODUCTION IONISATION PROCESSES. FRAGMENTATION PROCESSES. APPLICATIONS. ULTRAVIOLET AND VISIBLE SPECTROSCOPY. MOLECULAR ORBITAL AND ELECTRONIC TRANSITIONS. CHROMOPHORES. APPLICATIONS. INFRARED SPECTROSCOPY.
Teaching Methods
THE CLASS INCLUDES 32 HOURS OF LECTURES (4 CFU) AND 24 HOURS OF EXERCISES (2 CFU)
Verification of learning
THERE ARE TWO WRITTEN EXAMS DURING THE COURSE OR ONE AT THE END OF IT. THE WRITTEN EXAM IS PASSED IF THE GRADE IS AT LEAST 18/30. AFTER THE WRITTEN EXAM(S) THERE IS A DISCUSSION OF THE RESULTS (ORAL EXAM). THE GRADES OF THE WRITTEN EXAM(S) ARE USUALLY CONFRMED.
Texts
SILVERSTEIN, BASSLER E MORRIL, SPECTROMETRIC IDENTIFICATION OF ORGANIC COMPOUNDS, JOHN WILEY ED.
ROBERTS, GILBERT, MARTIN, CHIMICA ORGANICA SPERIMENTALE, ZANICHELLI ED.
STERNHELL, KALMAN, ORGANIC STRUCTURES FROM THEIR SPECTRA, JOHN WILEY ED. (1H-NMR SPECTRA)
SKOOG E LEARY, CHIMICA ANALITICA STRUMENTALE, EDISES (MASS SPECTROMETRY).
More Information
THE COURSE TEXT CAN BE FOUND IN THE DE RICCARDIS HOMEPAGE
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