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ADAVANCED ANALYTICAL CHEMISTRY

Ermanno VASCA ADAVANCED ANALYTICAL CHEMISTRY

0522300027
DEPARTMENT OF CHEMISTRY AND BIOLOGY "ADOLFO ZAMBELLI"
EQF7
CHEMISTRY
2017/2018



YEAR OF COURSE 2
YEAR OF DIDACTIC SYSTEM 2016
PRIMO SEMESTRE
CFUHOURSACTIVITY
648LESSONS
ERMANNO VASCA T Curriculum
Objectives
THE MAIN OBJECTIVES OF THE COURSE ARE:
(I)TO ASSESS KNOWLEDGE AND IMPROVE SKILLS IN APPLYING AND DEVELOPING METHODS FOR CHIMICA ANALYSIS
(II) TO DEVELOP THE ATTITUDE TO FACE ANALYTICAL PROBLEMS THROUGH LITERATURE SURVEY, CASE-STUDIES RESULTS AND CAREFUL INSTRUMENTAL MEASUREMENTS
Prerequisites
BACHELOR IN CHEMISTRY
Contents
PRESENTATION OF ADVANCED ANALYTICAL TECHNIQUES AND THEIR APPLICATION IN BOTH FUNDAMENTAL AND APPLIED ANALYTICAL CHEMISTRY.
PRINCIPLES, INSTRUMENTATION AND ANALYTICAL APPLICATIONS OF: VOLTAMMETRY, ELECTROGRAVIMETRY, COULOMETRY, AMPEROMETRY, SPECTROFLUORIMETRY, ATOMIC EMISSION SPECTROSCOPY, ICP-MS, GC-MS, LC-MS, IC-MS, SUPERCRITICAL CHROMATOGRAPHY, SIZE EXCLUSION CHROMATOGRAPHY, CAPILLARY ELECTROPHORESIS.
RADIOCHEMICAL METHODS OF ANALYSIS. ELEMENTAL ANALYSIS.
SENSORS. ION- SELECTIVE ELECTRODES. METHODS FOR THE DETERMINATION OF SELECTIVITY COEFFICIENTS. JUNCTION POTENTIALS. BIOSENSORS.
EQUILIBRIUM ANALYSIS AND SPECIATION. EXPERIMENTAL METHODS FOR THE DETERMINATION OF EQUILIBRIUM CONSTANTS. THE SPECIFIC INTERACTION THEORY.
ELECTRONIC SIGNALS AND NOISE.
DEVELOPMENT OF AN ANALYTICAL METHOD.
SAMPLING PRINCIPLES AND TECHNIQUES. SAMPLES PRE-TREATMENT METHODS. METHODS AND STATISTICAL PARAMETERS FOR THE ANALYTICAL PROTOCOL DEVELOPMENT. VALIDATION OF THE ANALYTICAL METHOD: SELECTIVITY, ROUGHNESS, PERCENT RECOVERY.
OFFICIAL METHODS FOR THE ANALYSIS OF CLINICAL, TOXICOLOGICAL, PHARMACEUTICAL, ENVIRONMENTAL, FOOD, AND MATERIALS SAMPLES.
HINTS IN CHEMIOMETRY.
PROCESS ANALYTICAL CHEMISTRY (CONTROL CHARTS, FLOW INJECTION ANALYSIS)
Teaching Methods
LECTURES
Verification of learning
ORAL EXAM
Texts
R. KELLNER, J.-M. MERMET, M. OTTO, M. VALCÁRCEL, H. M. WIDMER (EDS.)
ANALYTICAL CHEMISTRY
WILEY-VCH, NEW YORK, 2004

G. D. CHRISTIAN, “ANALYTICAL CHEMISTRY”, WILEY, NEW YORK, 2004

R. J. FLANAGAN, A. TAYLOR, I. D. WATSON, R. WHELPTON, FUNDAMENTALS OF ANALYTICAL TOXICOLOGY, WILEY, WEST SUSSEX, 2008

I. GRENTHE, I. PUIGDOMENECH (EDS.)
MODELLING IN AQUATIC CHEMISTRY
OECD PUBLICATIONS, PARIS, 1997
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