Paola RIZZO | TECHNIQUES OF MATERIALS CHARACTERIZATION AND LABORATORY
Paola RIZZO TECHNIQUES OF MATERIALS CHARACTERIZATION AND LABORATORY
cod. 0522300064
TECHNIQUES OF MATERIALS CHARACTERIZATION AND LABORATORY
| 0522300064 | |
| DEPARTMENT OF CHEMISTRY AND BIOLOGY "ADOLFO ZAMBELLI" | |
| EQF7 | |
| CHEMISTRY | |
| 2024/2025 |
| YEAR OF COURSE 2 | |
| YEAR OF DIDACTIC SYSTEM 2016 | |
| AUTUMN SEMESTER |
| SSD | CFU | HOURS | ACTIVITY | |
|---|---|---|---|---|
| CHIM/04 | 3 | 24 | LESSONS | |
| CHIM/04 | 3 | 36 | LAB |
| Objectives | |
|---|---|
| THE COURSE AIMS TO PROVIDE THEORETICAL AND PRACTICAL KNOWLEDGE OF THE MAIN MATERIALS CHARACTERIZATION TECHNIQUES THE STUDENT WILL KNOW AND HAVE DEVELOPED UNDERSTANDING OF THE FOLLOWING TOPICS: - X-RAY DIFFRACTION - THERMOGRAVIMETRIC ANALYSIS - DYNAMIC-MECHANICAL ANALYSIS - MECHANICAL ANALYSIS - DIFFERENTIAL SCANNING CALORIMETRY - INFRARED SPECTROSCOPY - BIREFRINGENCE THE STUDENT WITH THE KNOWLEDGE ACQUIRED, BOTH THEORETICAL AND PRACTICAL, WILL BE ABLE TO SELECT AND APPLY THE TECHNIQUES NECESSARY FOR THE STRUCTURAL CHARACTERIZATION OF MATERIALS THROUGH LABORATORY ANALYSIS, THE STUDENT WILL BECOME FAMILIAR WITH THE MATERIALS CHARACTERIZATION TECHNIQUES AND WILL BE LED TO GAIN AUTONOMY IN EVALUATING THE DEGREE OF EFFECTIVENESS AND INFORMATION OBTAINABLE FROM THEIR APPLICATION IN THE CONTEXT OF MATERIAL CHARACTERIZATION. THE STUDENT WILL BE ABLE TO COMMUNICATE THE KNOWLEDGE ACQUIRED DURING THE COURSE AND THE RESULTS OF THE LABORATORY EXPERIENCES, BOTH ORALLY AND THROUGH TEXTS OR VIRTUAL TOOLS, USING APPROPRIATE SCIENTIFIC TERMINOLOGY. THE STUDENT WILL BE ABLE TO: - UNDERSTAND AND INTERPRET BIBLIOGRAPHIC TEXTS ON DIFFERENT TYPES OF MATERIALS - PROCEED WITH THE CONTINUOUS UPDATING OF ONE'S KNOWLEDGE OF MATERIALS, USING TECHNICAL AND SCIENTIFIC LITERATURE. |
| Prerequisites | |
|---|---|
| A BASIC KNOWLEDGE OF POLYMER SCIENCE IS REQUIRED |
| Contents | |
|---|---|
| CONTENTS: -ORGANIZATION OF THE MATERIALS IN THE SOLID STATE: -THERMAL ANALYSIS (THERMOGRAVIMETRIC ANALYSIS (TGA), DIFFERENTIAL SCANNING CALORIMETRY ANALYSIS (DSC), DILATOMETRY, DYNAMIC-MECHANICAL ANALYSIS (DMA)) - MECHANICAL PROPERTIES (VISCOELASTICITY, STRESS-STRAIN CURVES) 1 CF / 8 HOURS - FRONTAL 1 CF / 12 HOURS - LABORATORY -AMORPHOUS STATE (GLASS TRANSITION (TG), PARAMETERS THAT INFLUENCE THE GLASS TRANSITION TEMPERATURE, TECHNIQUES TO DETERMINE THE GLASS TRANSITION TEMPERATURE) -CRYSTALLINE STATE (MORPHOLOGY, DEGREE OF CRYSTALLINITY, THERMODYNAMIC ASPECTS OF THE CRYSTALLIZATION OF POLYMERIC MATERIALS, CRYSTALLIZATION KINETICS, CORRELATION LENGTH OF THE CRYSTALLINE DOMAINS, SCHERRER EQUATION) -DIFFRAZIONE OF X-RAYS (PRODUCTION AND PROPERTIES OF X-RAY, ELEMENTS OF STRUCTURAL CHEMISTRY, BRAGG'S LAW, MEASUREMENT TECHNIQUES, EXAMPLES OF APPLICATION IN THE FIELD OF POLYMERS) 1 CF / 8 HOURS - FRONTAL 1 CF / 12 HOURS - LABORATORY -INFRARED SPECTROSCOPY (PRINCIPLES, SAMPLING TECHNIQUES, EXAMPLES IN THE POLYMERS FIELD) - MOLECULAR ORIENTATION (RX: HERMANS’ ORIENTATION FUNCTION, BIREFRINGENCE, INFRARED DICHROISM AND TRICHROISM) 1 CF / 8 HOURS - FRONTAL 1 CF / 12 HOURS - LABORATORY |
| Teaching Methods | |
|---|---|
| THE COURSE INCLUDES 60 HOURS OF TEACHING OF WHICH 24 HOURS OF LECTURES AND 36 HOURS OF LABORATORY EXPERIMENTS. CLASSROOM LESSONS WILL TAKE PLACE WITH THE AID OF PROJECTIONS AND ACCESS TO MULTIMEDIA MATERIAL FREELY AVAILABLE ONLINE. THE GUIDED EXERCISES IN THE MATERIALS CHARACTERIZATION LABORATORY INVOLVE ACTIVITIES GUIDED BY THE TEACHER ON THE MOST COMMON MATERIAL CHARACTERIZATION TECHNIQUES (X-RAY DIFFRACTION, THERMOGRAVIMETRY, DIFFERENTIAL SCANNING CALORIMETRY, DYNAMIC MECHANICAL ANALYSIS, ETC.). IN THE LABORATORY EXERCISES THE STUDENT WILL CARRY OUT EXPERIENCES WHERE THEY WILL HAVE TO PUT INTO PRACTICE AND VERIFY WHAT IS EXPLAINED IN THE LESSON. FOR THIS MODULE, ATTENDANCE IS MANDATORY FOR AT LEAST 75% OF THE TOTAL HOURS AND MUST BE EVIDENCED BY THE COMPILATION AND DELIVERY OF WRITTEN REPORTS TO THE TEACHER BEFORE TAKING THE EXAM |
| Verification of learning | |
|---|---|
| THE EXAM AIMS TO ENSURE THE STUDENT'S ACHIEVEMENT OF THE EDUCATIONAL OBJECTIVES PROPOSED IN THE COURSE. THE EXAM CONSISTS OF AN ORAL TEST. THE STUDENT WILL HAVE TO ANSWER A SERIES OF QUESTIONS THAT COVER ABOUT 75% OF THE TOPICS COVERED BY REFERRING TO THE LABORATORY EXERCISES CARRIED OUT. THE TEST ALSO INCLUDES THE DISCUSSION OF REPORT RELATING TO LABORATORY EXERCISES AND WILL BE AIMED AT VERIFYING THE STUDENT'S THEORETICAL KNOWLEDGE, WITH PARTICULAR REFERENCE TO THE ACHIEVEMENT OF THE TRAINING OBJECTIVES EXPLAINED IN THE DEDICATED SECTION. THE SCORE OF THE ORAL EXAM WILL DEPEND ON THE DEGREE OF ACCURACY OF THE REPORT, ON THE STUDENT'S ABILITY TO PRESENT THE TOPICS EXPLAINED IN THE CONTENTS SECTION EFFECTIVELY AND WITH RIGOROUS SCIENTIFIC LANGUAGE, ON THE MATURITY EXPRESSED BY THE STUDENT IN CRITICALLY DISCUSSING THE TOPICS ILLUSTRATED ALSO BY PROPOSING CONNECTIONS WITH THE CONTENTS OF OTHER TEACHINGS. THE STUDENT REACHES THE LEVEL OF EXCELLENCE IF HE OR SHE WILL BE ABLE TO TACKLE UNUSUAL PROBLEMS (OR THOSE NOT EXPRESSLY COVERED IN CLASS) AMONG THOSE PROPOSED IN THE ORAL EXAM. THE ORAL EXAM WILL LAST 30 MINUTES. THE TEST IS MARKED OUT OF THIRTIETH AND IS CONSIDERED PASSED WITH A MINIMUM MARK OF 18/30. |
| Texts | |
|---|---|
| SCIENZA E TECNOLOGIA DEI MATERIALI POLIMERICI DI BRUCKNER E ALLEGRA” EDIZIONE EDISES “FONDAMENTI DI SCIENZA DEI POLIMERI” A CURA DI M. GUAITA, F. CIARDELLI, F. LA MANTIA, E. PEDEMONTE, PACINI EDITORI. |
| More Information | |
|---|---|
| EMAIL:PRIZZO@UNISA.IT |
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