Anna Angela BARBA | CHEMICAL PLANTS
Anna Angela BARBA CHEMICAL PLANTS
cod. 0760400045
CHEMICAL PLANTS
| 0760400045 | |
| DIPARTIMENTO DI FARMACIA | |
| EQF7 | |
| PHARMACEUTICAL CHEMISTRY AND TECHNOLOGY | |
| 2024/2025 |
| YEAR OF COURSE 5 | |
| YEAR OF DIDACTIC SYSTEM 2023 | |
| AUTUMN SEMESTER |
| SSD | CFU | HOURS | ACTIVITY | |
|---|---|---|---|---|
| ING-IND/25 | 6 | 48 | LESSONS |
| Objectives | |
|---|---|
| THE COURSE AIMS TO PROVIDE KNOWLEDGE ON THE DEVELOPMENT AND THE DESIGN OF INDUSTRIAL PROCESSES AND PLANTS BY ADOPTING STANDARD AND INNOVATIVE TECHNOLOGIES (INTENSIFIED, SUSTAINABLE WITH REDUCED ENVIRONMENTAL IMPACT AND ORIENTED TOWARDS THE INDUSTRIAL AUTOMATION OF THE INDUSTRY 4.0), FOCUSING THE ATTENTION ON PRODUCTIONS OF CHEMISTRY AND OF PHARMACEUTICAL, NUTRACEUTICAL-FOOD AND BIOTECHNOLOGICAL SECTORS. KNOWLEDGE AND UNDERSTANDING AT THE END OF THE COURSE THE STUDENT WILL KNOW: - THE FUNDAMENTAL ELEMENTS OF PLANT LINES (PROCESS AND SERVICE), WITH EQUIPMENT AND INSTRUMENTATION TO MEASURE MAIN PROCESS VARIABLES; - THE TRANSPORT PHENOMENA INVOLVED IN TRANSFORMATION PROCESSES; - EXAMPLES OF INDUSTRIAL PROCESSES OF COMMON APPLICATION IN DIFFERENT INDUSTRIAL MANUFACTURING; - THE ELEMENTS OF INNOVATION FOR SUSTAINABLE, INTENSIFIED PROCESSES AND THE FUNDAMENTALS OF THE INDUSTRY 4.0 MANUFACTURING REVOLUTION BASED ON THE USE OF DIGITAL TECHNOLOGIES. MAKING JUDGMENTS AT THE END OF THE COURSE THE STUDENT WILL HAVE: ABILITY TO DEVELOP TRANSFORMATION PROCESSES BASIC SCHEMES, STARTING FROM THE IDENTIFICATION OF THE FUNDAMENTAL ELEMENTS, TO REACH MORE DETAILED PROCESS SCHEMES COMPREHENSIVE OF SUITABLE EQUIPMENT AND INSTRUMENTATION; ABILITY TO INDICATE THE KEY-PROCESSES INVOLVED IN PHARMACEUTICAL INDUSTRIAL TRANSFORMATIONS AND TO SUGGEST POSSIBLE INTERVENTIONS FOR GREATER PRODUCTION SUSTAINABILITY. |
| Prerequisites | |
|---|---|
| BASIC KNOWLEDGE OF CHEMISTRY, PHYSICS, MATHEMATICS |
| Contents | |
|---|---|
| INTRODUCTION TO THE PROGRAM CONTENTS; TEACHING AND EVALUATION METHODS; DIDACTIC MATERIALS. ELEMENTS OF METROLOGY: INTERNATIONAL SYSTEM – INRIM. THE ANATOMY OF A PRODUCTION PROCESS: BASIC PLANT ELEMENTS - REGULATION AND CONTROL EQUIPMENT AND TOOLS; PROCESS LINES AND ANCILLARY LINES. LAYOUT OF PRODUCTION LINES. REPRESENTATION WITH WORKFLOW AND PIPING AND INSTRUMENTATION DIAGRAM (PI&D). TECHNICAL-ECONOMIC ANALYSIS OF A PRODUCTION PROCESS. SYSTEM ANALYSIS: DESIGN PROBLEM, VERIFICATION PROBLEM. 4 HOURS INTRODUCTION TO THE MOST COMMON PROCESSES AND EQUIPMENT USED IN THE PHARMACEUTICAL FIELD REFERRING TO EXAMPLES OF PHARMACEUTICAL TRANSFORMATIONS INVOLVING HEAT TRANSFER, SIMULTANEOUS HEAT AND MASS TRANSFER. MODELS FOR THE STUDY OF UNIT OPERATIONS: EQUILIBRIUM STAGES MODEL, TRANSPORT PHENOMENA MODEL. FUNDAMENTALS OF MATERIAL AND ENERGY BALANCE. 4 HOURS HEAT EXCHANGE PROCESSES AND EQUIPMENT. SCHEMATIC REPRESENTATIONS. HEAT TRANSPORT PHENOMENA. EXCHANGE COEFFICIENTS. DESIGN EQUATION OF AN HEATER EXCHANGER. SCHEMATIC REPRESENTATIONS. 4 HOURS PROCESSES AND EQUIPMENT FOR CONCENTRATION BY SOLVENT EVAPORATION. SATURATED STEAM TABLE. SINGLE EFFECT - MULTIPLE EFFECTS EVAPORATORS WITH THERMAL RECOVERY. SCHEMATIC REPRESENTATIONS. 4 HOURS DRYING PROCESSES AND EQUIPMENT. DRYING METHODS, DRYING CURVES. AIR HYGROMETRY-USE OF HUMIDITY CHART. SCHEMATIC REPRESENTATIONS. 6 HOURS PROCESSES AND EQUIPMENT FOR OPERATIONS BASED ON EQUILIBRIUM STAGES. EQUILIBRIUM STAGE REPRESENTATION. LIQUID-SOLID AND LIQUID-LIQUID EXTRACTION: PHYSICAL PRINCIPLES. SCHEMATIC REPRESENTATIONS. DISTILLATION: PHYSICAL PRINCIPLES. SCHEMATIC REPRESENTATIONS. 6 HOURS PROCESSES AND EQUIPMENT FOR THE SIZE ENLARGEMENT OPERATION FOR GRANULAR AND POWDER MATERIALS FOR PHARMACEUTICAL USES. RELEVANCE IN THE PHARMACEUTICAL FIELD, PHYSICAL PRINCIPLES. FINAL TECHNOLOGICAL PROPERTIES OF THE PRODUCTS AND THEIR IMPACT ON STORAGE, DOSING AND TRANSPORT OPERATIONS (FLOWABILITY - FIFO, LIFO DISCHARGE MODELS). 6 HOURS GENERAL TECHNICAL SERVICES (BASIC UTILITIES) OF AN INDUSTRIAL PLANT: WATER, STEAM PRODUCTION, TECHNICAL GASES. 4 HOURS MEASUREMENT SYSTEMS OF THE MOST COMMON PROCESS VARIABLES: TEMPERATURE, FLOW, PRESSURE. CRITERIA FOR SUITABLE MEASUREMENT SYSTEMS SELECTION BASED ON TECHNICAL AND SAFETY ASPECTS. 6 HOURS INTRODUCTION TO PROCESS INTENSIFICATION: AIMS AND STRATEGIES. SUSTAINABLE AND RESPONSIBLE PRODUCTIONS: MEANING AND STRATEGIES. INDUSTRY 4.0. CONCLUSIVE REMARKS ON THE PRESENTED AND DISCUSSED TOPICS. 4 HOURS |
| Teaching Methods | |
|---|---|
| LECTURES IN CLASSROOM (48 HOURS, 6 CFU). |
| Verification of learning | |
|---|---|
| THE ACHIEVEMENT OF THE TEACHING OBJECTIVES WILL TAKE PLACE THROUGH AN ORAL INTERVIEW. IN PARTICULAR, THE ORAL EXAM CONSISTS OF THE DISCUSSION OF THE TOPICS PRESENTED IN LESSONS. THE AVERAGE DURATION RANGES FROM ABOUT TWENTY MINUTES (IN CASE OF ANSWERS GIVEN QUICKLY AND CORRECTLY), UP TO 40 MINUTES IF THE CANDIDATE HESITATE IN HIS ANSWERS AND NEEDS MORE TIME TO GIVE REASONED ANSWERS. THE OVERAL EVALUATION TAKES INTO CONSIDERATION THE SKILLS OF SYNTHESIS AND ANALYSIS IN THE DISCUSSION OF THE TOPICS REQUESTED AS WELL AS THE PROPERTIES OF TECHNICAL LANGUAGE. THE LEVEL OF SUFFICIENCY CORRESPONDS TO THE DEMONSTRATION OF THE ABILITY TO DESCRIBE THE FUNDAMENTAL ASPECTS OF THE DIFFERENT TOPICS OF THE TEACHING PROGRAM (PHYSICAL PRINCIPLES, CONSTRUCTION ASPECTS, FIELDS OF APPLICATION). THE LEVEL OF EXCELLENCE IS REACHED WHEN THE STUDENT PROVES ABLE TO SUCCESSFULLY DEAL WITH ASPECTS OF THE PROBLEMS NOT EXPLICITLY COVERED IN LESSONS, WITH TECHNICAL LANGUAGE. |
| Texts | |
|---|---|
| REFERENCE TEXTS: •HICKEY A.J.; GANDERTON D., PHARMACEUTICAL PROCESS ENGEERING, DRUG AND PHARMACEUTICAL SCIENCES VOL. 112, MARCEL DEKKER, INC. 2001 •FOUST AS, WENZEL LA, MAUS ANDERSEN I PRINCIPI DELLE OPERAZIONI UNITARIE, CASA EDITRICE AMBROSIANA BOLOGNA 1992 •COULSON AND RICHARDSON’S CHEMICAL ENGINEERING SERIES CHEMICAL ENGINEERING DESIGN SIXTH EDITION, RAY SINNOTT, GAVIN TOWLER, 2019 ELSEVIER BUTTERWORTH HEINEMANN CONSULTATION TEXTS: •PERRY’S CHEMICAL ENGINEERS’ HANDBOOK, MCGRAW HILL, NEW YORK, MCGRAW HILL; 9TH EDITION (AUGUST 29, 2018); ISBN-10: 0071834087; ISBN-13: 978-0071834087 •MCCABE W., SMITH., HARRIOT P., UNIT OPERATION OF CHEMICAL ENGINEERING, MCGRAW HILL, NEW YORK, 1993 •COULSON & RICHARDSON'S, CHEMICAL ENGINEERING, VOL. 1, FLUID FLOW, HEAT TRANSFER AND MASS TRANSFER, 6TH ED. 2001 ELSEVIER BUTTERWORTH HEINEMANN •MAGNANI G.A., FERRETTIG., ROCCO P., TECNOLOGIE DI SISTEMI DI CONTROLLO, SECONDA ED. 2007, MCGRAW-HILL OTHER •DIDACTIC MATERIAL WILL BE MADE AVAILABLE BY THE TEACHER AT THE LINK: HTTPS://DOCENTI.UNISA.IT/005842/RISORSE |
| More Information | |
|---|---|
| PLACE AND TIME. THE TEACHING IS DELIVERED AT THE DEPARTMENT OF PHARMACY; TIMETABLE AND CLASSROOM ARE AVAILABLE BY DEPARTMENT WEBSITE ( BY CDS WEB PAGES). |
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