Francesco DE RICCARDIS | ADVANCED TOPICS IN ORGANIC CHEMISTRY
Francesco DE RICCARDIS ADVANCED TOPICS IN ORGANIC CHEMISTRY
cod. 8803300012
ADVANCED TOPICS IN ORGANIC CHEMISTRY
| 8803300012 | |
| DEPARTMENT OF CHEMISTRY AND BIOLOGY "ADOLFO ZAMBELLI" | |
| P.H.D. COURSE | |
| CHEMICAL, BIOLOGICAL AND ENVIRONMENTAL SCIENCES | |
| 2022/2023 |
| OBBLIGATORIO | |
| YEAR OF COURSE 3 | |
| YEAR OF DIDACTIC SYSTEM 2020 | |
| AUTUMN SEMESTER |
| SSD | CFU | HOURS | ACTIVITY | ||
|---|---|---|---|---|---|
| CHIMICA DEI COMPOSTI ETEROCICLICI | |||||
| CHIM/06 | 0.5 | 4 | LESSONS | ||
| FOTOCATALISI IN SINTESI ORGANICA | |||||
| CHIM/06 | 0.5 | 4 | LESSONS | ||
| Objectives | |
|---|---|
| THE COURSE, CONSISTING OF CLASS LECTURES, AIMS TO PROVIDE KNOWLEDGE OF PHOTO-CATALYSIS FIELD AND ITS USE IN ORGANIC SYNTHESIS WITH PARTICULAR EMPHASIS ON ASYMMETRIC SYNTHESIS. MOREOVER, PURPOSE OF THE COURSE IS TO GIVE INFORMATION ABOUT THE MOST USED METHODS FOR THE SYNTHESIS OF INTERESTING HETEROCYCLIC COMPOUNDS. THE MAIN ACQUIRED KNOWLEDGE WILL BE: •ASYMMETRIC METAL-FREE PHOTOCATALYSIS •SYNTHETIC APPROACH TOWARDS SEVERAL CLASSES OF HETEROCYCLIC POLYPHENOLIC COMPOUNDS. THE MAIN SKILLS WILL BE: •TO DESIGN THE SYNTHESIS OF HETEROCYCLIC COMPOUNDS (ON SOLID-PHASE, TOO). •TO SOLVE SYNTHETIC PROBLEMS USING PHOTO-CATALYTIC METHODOLOGIES. |
| Prerequisites | |
|---|---|
| FUNDAMENTALS OF ORGANIC CHEMISTRY I AND II. |
| Contents | |
|---|---|
| MECHANISM OF PHOTOCATALYTIC REACTIONS IN ASYMMETRIC SYNTHESIS APPLICATION TO THE SYNTHESIS OF BIOACTIVE PRODUCTS DESCRIPTION OF SYNTHETIC METHODS AND TRANSFORMATION OF COUMARINS, FLAVONES, STYRYLCHROMONES, ISOFLAVONES, ANTHOCYANINS, XANTHONES, TANNINS. SOLID-PHASE SYNTHESIS OF PEPTIDES AND OLIGONUCLEOTIDES. RESINS, CONDENSING AGENTS, PROTECTIVE GROUPS. PROBLEMS OF MODERN SYNTHESIS ON SOLID PHASE |
| Teaching Methods | |
|---|---|
| THE TEACHING WILL BE 8 HOURS OF CLASSROOM LESSONS AND POWERPOINT PRESENTATIONS. THERE WILL BE PDF FILES AVAILABLE TO THE ATTENDING STUDENTS. |
| Verification of learning | |
|---|---|
| ORAL EXAMINATION WILL BE HELD, CONSISTING OF A DISCUSSION ABOUT A RESEARCH PAPER CONCERNING THE SUBJECT OF THE COURSE. |
| Texts | |
|---|---|
| •NEW FRONTIERS IN ASYMMETRIC CATALYSIS, MIKAMI, K., LAUTENS, M., EDS. WILEY-VCH, 2007. •ASYMMETRIC ORGANOCATALYSIS, BERKESSEL A., GRÖGER. H., ED., WILEY-VCH, 2005. •VISIBLE LIGHT PHOTOCATALYSIS IN ORGANIC CHEMISTRY, STEPHENSON, C.; YOON, T.; MACMILLAN, D. W. C., WILEY-VCH, 2018. •THE FLAVONOIDS: ADVANCES IN RESEARCH SINCE 1986, J. B. HARBORNE,EDITOR. CHAPMAN & HALL: NEW YORK, NY, 1994 •“ARYLXANTHONES AND ARYLACRIDONES: A SYNTHETIC OVERVIEW”, CLEMENTINA M. M. SANTOS, DIANA C. G. A. PINTO, VERA L. M. SILVA, ARTUR M. S. SILVA, PURE APPL. CHEM., 2016; 88, 579-594. •“AN OVERVIEW OF 2-STYRYLCHROMONES: NATURAL OCCURRENCE, SYNTHESIS, REACTIVITY AND BIOLOGICAL PROPERTIES”, CLEMENTINA M. M. SANTOS, ARTUR M. S. SILVA, EUR. J. ORG. CHEM., 2017, 3115-3133. •“SYNTHESIS OF ENANTIOPURE 2-C-GLYCOSYL-3-NITROCHROMENES”, RAQUEL G. SOENGAS, HUMBERTO RODRÍGUEZ-SOLLA, ARTUR M. S. SILVA, RICARDO LLAVONA, FILIPE A. ALMEIDA PAZ, J. ORG. CHEM., 2013, 78, 1283112836. |
| More Information | |
|---|---|
| MORE INFORMATION WILL BE AVAILABLE BY E-MAIL: GDSALA@UNISA.IT, DERICCA@UNISA.IT |
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