FOUNDATIONS OF ANALYTICAL CHEMISTRY

RAFFAELE CUCCINIELLO FOUNDATIONS OF ANALYTICAL CHEMISTRY

0512400013
DEPARTMENT OF CHEMISTRY AND BIOLOGY "ADOLFO ZAMBELLI"
EQF6
CHEMISTRY
2019/2020

OBBLIGATORIO
YEAR OF COURSE 1
YEAR OF DIDACTIC SYSTEM 2016
SECONDO SEMESTRE
CFUHOURSACTIVITY
648LESSONS
112EXERCISES
560LAB
Objectives
THE AIM OF THE COURSE IS TO QUALIFY IN PERFORMING ANALYTICAL DETERMINATIONS USING CLASSICAL METHODS OF ANALYSIS (TITRIMETRIC AND GRAVIMETRIC) AND TO PROPERLY UNDERSTAND ANALYTICAL PROTOCOLS.
Prerequisites
FUNDAMENTALS OF GENERAL CHEMISTRY, MATHEMATICS, PHYSICS, INFORMATICS AND ENGLISH LANGUAGE
Contents
BASIC TOOLS AND OPERATIONS OF ANALYTICAL CHEMISTRY. THE MAIN STEPS IN A CHEMICAL ANALYSIS. (5 HOURS)
ERRORS IN ANALYTICAL DETERMINATIONS. DATA HANDLING AND SPREADSHEETS IN ANALYTICAL CHEMISTRY. (5 HOURS)
ACID-BASE EQUILIBRIA IN CHEMICAL ANALYSIS. GRAPHICAL AND NUMERICAL METHODS FOR THE STUDY AND THE INTERPRETATION OF ACID-BASE EQUILIBRIA. APPLICATION OF ACID-BASE REACTIONS FOR QUANTITATIVE AND QUALITATIVE ANALYSIS. (20 HOURS, 15 HOURS LABORATORY)
COMPLEX FORMATION EQUILIBRIA IN CHEMICAL ANALYSIS. GRAPHICAL AND NUMERICAL METHODS FOR THE STUDY AND THE INTERPRETATION OF COMPLEX FORMATION EQUILIBRIA. APPLICATION OF COMPLEX FORMATION REACTIONS FOR QUANTITATIVE AND QUALITATIVE ANALYSIS. (10 HOURS, 15 HOURS LABORATORY)
REDOX EQUILIBRIA IN CHEMICAL ANALYSIS. GRAPHICAL AND NUMERICAL METHODS FOR THE STUDY AND THE INTERPRETATION OF REDOX EQUILIBRIA. APPLICATION OF REDOX REACTIONS FOR QUANTITATIVE AND QUALITATIVE ANALYSIS. (10 HOURS, 15 HOURS LABORATORY)
SOLUBILITY EQUILIBRIA IN CHEMICAL ANALYSIS. GRAPHICAL AND NUMERICAL METHODS FOR THE STUDY AND THE INTERPRETATION OF SOLUBILITY EQUILIBRIA. APPLICATION OF PRECIPITATION REACTIONS FOR QUANTITATIVE AND QUALITATIVE ANALYSIS. (10 HOURS, 15 HOURS LABORATORY)

Teaching Methods
LECTURES (6 CFU, 48 HOURS); NUMERICAL EXAMPLES (1 CFU, 12 HOURS); LABORATORY WORK (5 CFU, 60 HOURS).
Verification of learning
WRITTEN AND ORAL EXAM
Texts
F. J. HOLLER, S. R. CROUCH, SKOOG AND WEST’S FUNDAMENTALS OF ANALYTICAL CHEMISTRY, 9TH ED., BROOKS/COLE CENGAGE LEARNING, 2014

D. C. HARRIS, QUANTITATIVE CHEMICAL ANALYSIS, 8TH ED., W. H. FREEMAN AND CO., NEW YORK, 2010

L. CIAVATTA, LEZIONI DI CHIMICA ANALITICA, LIGUORI, NAPOLI, 1995
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