Stefania PRAGLIOLA | LABORATORY OF CHEMISTRY

cod. 0512700008

LABORATORY OF CHEMISTRY

	0512700008
	DEPARTMENT OF CHEMISTRY AND BIOLOGY "ADOLFO ZAMBELLI"
	EQF6
	ENVIRONMENTAL SCIENCES
	2018/2019

PERCORSO COMUNE

	OBBLIGATORIO
	YEAR OF COURSE 1
	YEAR OF DIDACTIC SYSTEM 2016
	ANNUALE

TEACHING UNITS

	SSD	CFU	HOURS	ACTIVITY	TYPE OF ACTIVITY
1	LABORATORIO DI CHIMICA GENERALE E INORGANICA (MODULO DI LABORATORIO DI CHIMICA)
	CHIM/03	2	16	LESSONS	BASIC COMPULSORY SUBJECTS
	CHIM/03	1	12	LAB	BASIC COMPULSORY SUBJECTS
	CHIM/03	1	12	EXERCISES	BASIC COMPULSORY SUBJECTS
2	LABORATORIO DI CHIMICA ORGANICA (MODULO DI LABORATORIO DI CHIMICA)
	CHIM/06	1	12	LAB	BASIC COMPULSORY SUBJECTS
	CHIM/06	1	12	EXERCISES	BASIC COMPULSORY SUBJECTS

PROFESSORS

	IRENE IZZO2 T Curriculum
	STEFANIA PRAGLIOLA1 Curriculum
	CARMINE CAPACCHIONE1 Curriculum
	GIORGIO DELLA SALA2 Curriculum

	Objectives
	LEARNING OF ADEQUATE KNOWLEDGE ON THE LABORATORY SAFETY PROCEDURES AND RULES AND LABORATORY PRACTICE OF INORGANIC AND ORGANIC CHEMISTRY. ACQUISITION OF METHODOLOGIES FOR THE SYNTHESIS OF INORGANIC COMPOUNDS AND METHODS FOR ISOLATION AND PURIFICATION OF ORGANIC AND INORGANIC COMPOUNDS.

	Prerequisites
	THE STUDENT MUST HAVE ACQUIRED THE BASIC KNOWLEDGE IN THE FIELD OF CHEMISTRY PROVIDED BY THE NORMAL HIGH SCHOOL STUDY PROGRAMS.

	Contents
	AFTER AN INTRODUCTORY PART CONCERNING THE CHEMICAL LABORATORY SAFETY ELEMENTS AND AN INTRODUCTION TO THE SAFETY REGULATIONS ON THE LABELING OF CHEMICAL REAGENTS (24 HOURS), CONCERNING THE PART OF THE LABORATORY OF CHEMISTRY RELATED TO GENERAL CHEMISTRY: TUTORIALS: EXERCISES OF STOICHIOMETRY (12 HOURS) LABORATORY PRACTICES: DETERMINATION OF THE MOLECULAR WEIGHT OF A VOLATILE LIQUID. SYNTHESIS OF SODIUM CARBONATE ACCORDING TO THE SOLVAY METHOD. SYNTHESIS OF IRON OXIDES (II) AND IRON (III). CONCERNING THE PART OF THE LABORATORY OF CHEMISTRY RELATED TO ORGANIC CHEMISTRY: -TUTORIALS: EXERCISES ON SYSTEMATIC NOMENCLATURE, STRUCTURES, CHEMICAL-PHYSICS PROPERTIES BASIC PRINCIPLES OF REACTIVITY OF THE MOST COMMON CLASSES OF ORGANIC COMPOUNDS: ALKANES, ALKENES, ALKYNES, ALKYL HALIDES, ALCOHOLS, ALDEHYDES, KETONES, BENZENE AND DERIVATIVES, AMINES, CARBOXYLIC ACIDS AND DERIVATIVES. (12 HOURS) LABORATORY PRACTICES: CRYSTALLIZATION OF BENZOIC ACID (4 HOURS) EXTRACTION AND CHROMATOGRAPHY OF PHOSOSYNTHETIC PIGMENTS OF CLOOPHILLA FROM SPINACH LEAVES.(4 HOURS) EXTRACTION OF CAFFEINE FROM TEA LEAVES. (4 HOURS)

AFTER AN INTRODUCTORY PART CONCERNING THE CHEMICAL LABORATORY SAFETY ELEMENTS AND AN INTRODUCTION TO THE SAFETY REGULATIONS ON THE LABELING OF CHEMICAL REAGENTS (24 HOURS), CONCERNING THE PART OF THE LABORATORY OF CHEMISTRY RELATED TO GENERAL CHEMISTRY:

TUTORIALS: EXERCISES OF STOICHIOMETRY (12 HOURS)

LABORATORY PRACTICES:
DETERMINATION OF THE MOLECULAR WEIGHT OF A VOLATILE LIQUID.
SYNTHESIS OF SODIUM CARBONATE ACCORDING TO THE SOLVAY METHOD.
SYNTHESIS OF IRON OXIDES (II) AND IRON (III).

CONCERNING THE PART OF THE LABORATORY OF CHEMISTRY RELATED TO ORGANIC CHEMISTRY:

-TUTORIALS: EXERCISES ON SYSTEMATIC NOMENCLATURE, STRUCTURES, CHEMICAL-PHYSICS PROPERTIES BASIC PRINCIPLES OF REACTIVITY OF THE MOST COMMON CLASSES OF ORGANIC COMPOUNDS: ALKANES, ALKENES, ALKYNES, ALKYL HALIDES, ALCOHOLS, ALDEHYDES, KETONES, BENZENE AND DERIVATIVES, AMINES, CARBOXYLIC ACIDS AND DERIVATIVES. (12 HOURS)

LABORATORY PRACTICES:
CRYSTALLIZATION OF BENZOIC ACID (4 HOURS)
EXTRACTION AND CHROMATOGRAPHY OF PHOSOSYNTHETIC PIGMENTS OF CLOOPHILLA FROM SPINACH LEAVES.(4 HOURS)
EXTRACTION OF CAFFEINE FROM TEA LEAVES. (4 HOURS)

	Teaching Methods
	THE COURSE INCLUDES 72 HOURS OF TEACHING BETWEEN THE LABORATORY AND TUTORIALS. IN PARTICULAR, THERE ARE 48 HOURS OF CLASSROOM EXERCISES AND LESSONS (4CFU) AND 24 HOURS OF GUIDED LABORATORY PRACTICES (4 CFUS). THE COURSE IS ORGANIZED AS FOLLOWS: STOICHIOMETRY AND ORGANIC CHEMISTRY TUTORIALS AND LABORATORY SAFETY LESSONS WILL PRECEDE THE PRACTICAL PART IN THE LAB. STUDENTS WILL BE DIVIDED INTO GROUPS (MAXIMUM 3 STUDENTS/GROUP) AND WILL FOLLOW 6 GUIDED LABORATORY PRACTICES OF 4 HOURS EACH. AT THE END OF THE LABORATORY PRACTICES, STUDENTS WILL HAVE TO WRITE A REPORT ABOUT THE EXPERIENCE AND COMMENT ON THE RESULTS OBTAINED. LABORATORY ATTENDANCE IS MANDATORY WITH A MAXIMUM OF10% (1 EXPERIENCE) OF ABSENCE.

Teaching Methods

THE COURSE INCLUDES 72 HOURS OF TEACHING BETWEEN THE LABORATORY AND TUTORIALS. IN PARTICULAR, THERE ARE 48 HOURS OF CLASSROOM EXERCISES AND LESSONS (4CFU) AND 24 HOURS OF GUIDED LABORATORY PRACTICES (4 CFUS).
THE COURSE IS ORGANIZED AS FOLLOWS:
STOICHIOMETRY AND ORGANIC CHEMISTRY TUTORIALS AND LABORATORY SAFETY LESSONS WILL PRECEDE THE PRACTICAL PART IN THE LAB. STUDENTS WILL BE DIVIDED INTO GROUPS (MAXIMUM 3 STUDENTS/GROUP) AND WILL FOLLOW 6 GUIDED LABORATORY PRACTICES OF 4 HOURS EACH. AT THE END OF THE LABORATORY PRACTICES, STUDENTS WILL HAVE TO WRITE A REPORT ABOUT THE EXPERIENCE AND COMMENT ON THE RESULTS OBTAINED.
LABORATORY ATTENDANCE IS MANDATORY WITH A MAXIMUM OF10% (1 EXPERIENCE) OF ABSENCE.

	Verification of learning
	THE ACHIEVEMENT OF THE OBJECTIVES OF THE COURSE IS CERTIFIED BY PASSING AN EVALUATION EXAM WITH THE MAXIMUM FINAL NOTE IN 30/30. THE EXAM INVOLVES THE PREPARATION OF A DETAILED WRITTEN REPORT FOR EACH LABORATORY EXPERIENCE AND THE ORAL DISCUSSION OF THE BACKGROUND PRINCIPLES OF THE LABORATORY PRACTICE AND A DETAILED DISCUSSION OF THE RESULTS OBTAINED.THE HONORS WILL BE AWARDED TO THE STUDENT WHO WORKED SERIOUSLY AND FAULTLESS IN THE LABORATORY AND PRESENTS THE TOPICS COVERED FULLY, IN AN ERROR-FREE AND EXCELLENT WAY.

Verification of learning

THE ACHIEVEMENT OF THE OBJECTIVES OF THE COURSE IS CERTIFIED BY PASSING AN EVALUATION EXAM WITH THE MAXIMUM FINAL NOTE IN 30/30. THE EXAM INVOLVES THE PREPARATION OF A DETAILED WRITTEN REPORT FOR EACH LABORATORY EXPERIENCE AND THE ORAL DISCUSSION OF THE BACKGROUND PRINCIPLES OF THE LABORATORY PRACTICE AND A DETAILED DISCUSSION OF THE RESULTS OBTAINED.THE HONORS WILL BE AWARDED TO THE STUDENT WHO WORKED SERIOUSLY AND FAULTLESS IN THE LABORATORY AND PRESENTS THE TOPICS COVERED FULLY, IN AN ERROR-FREE AND EXCELLENT WAY.

	Texts
	FONDAMENTI DI STECHIOMETRIA, M. GIOMINI, E. BALESTRIERI, M. GIUSTINI, EDISES (NAPOLI) STECHIOMETRIA, I. BERTINI, C. LUCHINAT, F. BERTINI CASA EDITRICE AMBROSIANA STUDENT SOLUTION MANUAL - INTRODUCTION TO ORGANIC CHEMISTRY (IV EDITION), F.S. LEE, W. BROWN, T. POON, JOHN WILEY & SONS, INC; EXPERIMENTAL ORGANIC CHEMISTRY, R. M. ROBERTS; J. C. GILBERT; S. F. MARTIN; LECTURE NOTES.

	More Information
	ADDITIONAL INFORMATION MAY BE REQUESTED FOR THE TEACHERS OF THE COURSE: CARMINE CAPACCHIONE: CCAPACCHIONE@UNISA.IT IRENE IZZO: IIZZO@UNISA.IT

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Stefania PRAGLIOLA | LABORATORY OF CHEMISTRY